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-{{Infobox chemical analysis
+== Trinidad Tobago Hollister Shop Doncaster ==
-| name = Thermogravimetric analysis
-| acronym = TGA
-| classification =[[Thermal analysis]]
-<gallery>
+The GPS signal sent by satellite includes by design a diploma of builtin inaccuracy. GPS was created for the military. This builtin error is supposed to prevent an enemy from using GPS to target friendly forces with a high degree of precision. The north of Scotland will be fresher and could hold on to mainly dry conditions with a few sunshine for much of the period. There is a possibility of the weather gradually increasingly settled from the southwest right at the end of next week. Probably still rather warm in the south at first but temperatures are expected to fall to nearer normal in most areas, with a cooler feel under cloud and rain, especially initially in the east.. <br><br>Choose rutabagas which are heavy to the hand; store these questions cool, dark place for a month or so. The skin is edible  provided it's thin and tender. S could be eaten raw, shredded or diced in salads, used as a vehicle for fullflavored dips, or cooked any way you'd cook a potato. <br><br>The room was impressive, and the kitchenette having a fullsize fridge was lovely. If only we had time to actually utilize it [http://www.ivplaster.com.au/images/inches/breit.asp?l=56-Hollister-Shop-Doncaster Hollister Shop Doncaster] (we left early in the day and came back late at night). The pillows were AMAZING. Locksmiths are utilized all throughout the world. Every country has their particular set of standards when it comes to locksmiths. Some locksmiths have to be subjected to severe security checks while others are able to practice with ease. <br><br>Conditions change. Trails might be closed because of logging operations. Bridges wash out, trees fall, ice melts, and property owners rescind their permission to use their land. Creekside Commerce park is on the south side of Immokalee Road. The largest chunk of vacant land around the block is [http://www.weddingsbyjohn.com.au/SpryAssets/vertical.asp?r=22-Ray-Ban-Sale Ray Ban Sale] on the east side of GoodletteFrank Road. That's where Barron Collier Cos. <br><br>Third  the taxation of software transactions, isn't yet fully certain for suppliers of software from treaty jurisdictions, many of whose tax treaties with India drafted long ago in [http://www.ivplaster.com.au/images/inches/breit.asp?l=91-Hollister-Co-Doncaster Hollister Co Doncaster] the 1980s and 1990s, don't explicitly envisage tax on software underneath the definition of "Royalty" in such treaties [for example, tax treaties with US, UK, Singapore, Japan, Australia, and many more]. On the [http://www.slickwebsites.com.au/images/test/test.asp?k=65-Replica-Oakley-Holbrook Replica Oakley Holbrook] contrary, there are treaties with Malaysia, Russia, Trinidad Tobago, Turkmenistan, Namibia and Morocco, etc, where taxation of computer software is specifically envisaged underneath the "Royalty" article of the treaty. While the position on these latter countries is apparent, the question is about the fate of suppliers from the former jurisdictions, and equally of Indian companies who've acquired software from such jurisdictions? Will the wages Tax Department argue in the court that the amended definition of Section 9(1)(vi) extends to all of India's tax treaties although the definition of "Royalties" under such treaties did not specifically cover software transactions? You might hope that India would honor the treaty definitions and not seek to override treaties with this domestic law change.<ul>
-Image:Thermogravimetric analyser.jpg|A typical TGA system
-</gallery>
+   <li>[http://danengyili.com/forum.php?mod=viewthread&tid=590310 http://danengyili.com/forum.php?mod=viewthread&tid=590310]</li>
-| analytes =
-| manufacturers =
+   <li>[http://myextremeauto.com/activity/p/19022/ http://myextremeauto.com/activity/p/19022/]</li>
-| related = [[Isothermal microcalorimetry]]<br>[[Differential scanning calorimetry]]<br>[[Dynamic mechanical analysis]]<br>[[Thermomechanical analysis]]<br>[[Differential thermal analysis]]<br>[[Dielectric thermal analysis]]
-| hyphenated =
+   <li>[http://www.imnic.net/forum.php?mod=viewthread&tid=50635 http://www.imnic.net/forum.php?mod=viewthread&tid=50635]</li>
-}}
+   <li>[http://globetee.com/courses/sentosa-golf-club?page=480#comment-24021 http://globetee.com/courses/sentosa-golf-club?page=480#comment-24021]</li>
+ </ul>
-'''Thermogravimetric analysis''' or '''thermal gravimetric analysis''' (TGA) is a method of [[thermal analysis]] in which changes in physical and chemical properties of materials are measured as a function of increasing temperature (with constant heating rate), or as a function of time (with constant temperature and/or constant mass loss).<ref name=ref1>{{cite journal | title = Thermogravimetric Analysis: A Review | journal = [[Analyst (journal)|Analyst]] | year = 1963 | volume = 88 | pages = 906–924 | doi = 10.1039/AN9638800906 | author1 = Coats, A. W. | author2 = Redfern, J. P.|bibcode = 1963Ana....88..906C }}</ref>  TGA can provide information about physical phenomena, such as [[second-order phase transition]]s, including [[vaporization]], [[sublimation (phase transition)|sublimation]], [[absorption (chemistry)|absorption]], [[adsorption]], and [[desorption]].  Likewise, TGA can provide information about chemical phenomena including [[chemisorption]]s, [[desolvation]] (especially [[dehydration]]), [[decomposition]], and solid-gas reactions (e.g., [[oxidation]] or [[redox|reduction]]).<ref name=ref1>{{cite journal | title = Thermogravimetric Analysis: A Review | journal = [[Analyst (journal)|Analyst]] | year = 1963 | volume = 88 | pages = 906–924 | doi = 10.1039/AN9638800906 | author1 = Coats, A. W. | author2 = Redfern, J. P.|bibcode = 1963Ana....88..906C }}</ref>
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-TGA is commonly used to determine selected characteristics of materials that exhibit either mass loss or gain due to decomposition, oxidation, or loss of [[volatiles]] (such as moisture).  Common applications of TGA are (1) materials characterization through analysis of characteristic decomposition patterns, (2) studies of degradation mechanisms and reaction kinetics, (3) determination of organic content in a sample, and (4) determination of inorganic (e.g. ash) content in a sample, which may be useful for corroborating predicted material structures or simply used as a chemical analysis.  It is an especially useful technique for the study of [[polymer]]ic materials, including [[thermoplastics]], [[thermosets]], [[elastomers]], [[composite material|composites]], [[plastic film]]s, [[fibers]], [[coatings]] and [[paints]].  Discussion of the TGA apparatus, methods, and trace analysis will be elaborated upon below. Thermal stability, oxidation, and combustion, all of which are possible interpretations of TGA traces, will also be discussed.
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-==Instrumental apparatus==
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-Though a constant heating rate is more common, a constant mass loss rate can illuminate specific reaction kinetics. For example, the kinetic parameters of the carbonization of polyvinyl butyral were found using a constant mass loss rate of 0.2 wt %/min.<ref name=ref2>{{cite journal | title = Carbonization of polymeric nonwoven materials | journal = [[Thermochimica Acta]] | year = 2009 | volume = 486 | pages = 66–70 | doi = 10.1016/j.tca.2008.12.020 | author1 = Tikhonov, N. A. | author2 = Arkhangelsky, I. V. | author3 = Belyaev, S. S. | author4 = Matveev, A. T.}}</ref>  Regardless of the furnace programming, the sample is placed in a small, electrically heated furnace equipped with a [[thermocouple]] to monitor accurate measurements of the temperature by comparing its voltage output with that of the voltage-versus-temperature table stored in the computer’s memory. A reference sample may be placed on another balance in a separate chamber. The atmosphere in the sample chamber may be purged with an [[inert gas]] to prevent oxidation or other undesired reactions. A different process using a quartz crystal microbalance has been devised for measuring smaller samples on the order of a microgram (versus milligram with conventional TGA).<ref name=ref3>{{cite web | title = Thermogravimetric Analysis | url = http://vedyadhara.ignou.ac.in/wiki/images/1/1c/UNIT_10_THERMOGRAVIMETRIC_ANALYSIS.pdf}}</ref> Figure 1 provides schematic diagrams of a typical TGA instrument.
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-The TGA instrument continuously weighs a sample as it is heated to temperatures of up to 2000°C for coupling with [[FTIR]] and [[Mass spectrometry]] gas analysis. As the temperature increases, various components of the sample are decomposed and the weight percentage of each resulting mass change can be measured. Results are plotted with temperature on the X-axis and mass loss on the Y-axis. The data can be adjusted using curve smoothing and first derivatives are often also plotted to determine points of inflection for more in-depth interpretations (see discussion on Trace Analysis).
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-* A horizontal portion, or plateau that indicates constant sample weight (Regions A and C in Figure 2)
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-* A curved portion; the steepness of the curve indicates the rate of mass loss (Region B in Figure 2)
-* An inflection (at which <math>\frac{dw}{dt}</math> is a minimum, but not zero)
-Certain features in the TGA curve that are not readily seen can be more clearly discerned in the first derivative TGA curve.  For example, any change in the rate of weight loss can immediately be seen in the first derivative TGA curve as a trough, or as a shoulder or tail to the peak, indicating two consecutive or overlapping reactions.  Differential TGA curves also can show considerable similarity to [[differential thermal analysis]] (DTA) curves, which can permit easy comparisons to be made.<ref name=ref1>{{cite journal | title = Thermogravimetric Analysis: A Review | journal = [[Analyst]] | year = 1963 | volume = 88 | pages = 906–924 | doi = 10.1039/AN9638800906 | author1 = Coats, A. W. | author2 = Redfern, J. P.|bibcode = 1963Ana....88..906C }}</ref>
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-Metal aluminates (MAl<sub>2</sub>O<sub>4</sub>) are an important type of mixed-cation oxide ceramics that have many applications.<ref name=ref5>{{cite journal | title = Synthesis and Characterization of Precursors for Group II Metal Aluminates | journal = [[Appl. Organomet. Chem.]] | year = 1997 | volume = 11 | pages = 919–927 | doi = 10.1002/(SICI)1099-0739(199710/11)11:10/11<919::AID-AOC666>3.0.CO;2-Z | author1 = Narayanan, R. | author2 = Laine, R. M.}}</ref>  The metal aluminate CaAl<sub>2</sub>O<sub>4</sub> is used in the cement industry as a hydraulic material.<ref name=ref5>{{cite journal | title = Synthesis and Characterization of Precursors for Group II Metal Aluminates | journal = [[Appl. Organomet. Chem.]] | year = 1997 | volume = 11 | pages = 919–927 | doi = 10.1002/(SICI)1099-0739(199710/11)11:10/11<919::AID-AOC666>3.0.CO;2-Z | author1 = Narayanan, R. | author2 = Laine, R. M.}}</ref>  The TGA of the precursor to calcium aluminate CaAl<sub>2</sub>C<sub>18</sub>H<sub>37</sub>O<sub>9</sub>N<sub>3</sub> is shown in Figure 3.<ref name=ref5>{{cite journal | title = Synthesis and Characterization of Precursors for Group II Metal Aluminates | journal = [[Appl. Organomet. Chem.]] | year = 1997 | volume = 11 | pages = 919–927 | doi = 10.1002/(SICI)1099-0739(199710/11)11:10/11<919::AID-AOC666>3.0.CO;2-Z | author1 = Narayanan, R. | author2 = Laine, R. M.}}</ref> The formation of CaAl2O4 occurs during the thermogravimetric analysis. This is how the theoretical ceramic yield is calculated for this example:
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-(1) Calculate molecular weight of CaAl<sub>2</sub>O<sub>4</sub>:
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-       <math> 40.078 + (2*26.982) + (4*15.999) = 158.038 g/mol </math>
-(2) Calculate molecular weight of CaAl<sub>2</sub>C<sub>18</sub>H<sub>37</sub>O<sub>9</sub>N<sub>3</sub>:
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-       <math> 40.078 +(2*26.982) + (18*12.011) + (37*1.008) + (9*15.999) + (3*14.007) = 533.548 g/mol </math>
-(3) Calculate the percentage that CaAl<sub>2</sub>O<sub>4</sub> is of CaAl<sub>2</sub>C<sub>18</sub>H<sub>37</sub>O<sub>9</sub>N<sub>3</sub>:
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-       <math>\frac{molecular weight of CaAl2O4}{molecular weight of CaAl2C18H37O9N3} * 100 = \frac{158.038 g/mol}{533.548 g/mol} * 100 = 29.6% </math>
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-Therefore, the theoretical ceramic yield for the thermogravimetric analysis of  CaAl<sub>2</sub>C<sub>18</sub>H<sub>37</sub>O<sub>9</sub>N<sub>3</sub> is 29.6%. This correlates well with the experimentally determined ceramic yield of 28.9%.
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-As another example of calculating theoretical ceramic yield, the TGA of calcium oxalate monohydrate is shown in Figure 4. Using the same process detailed above, the theoretical ceramic yield can be calculated: the formula weight of calcium oxalate monohydrate is 146 g/mol. The final ceramic product is CaO, with a formula weight of 56 g/mol. The theoretical ceramic yield is therefore 38.4%.  The actual yield from the TGA was found to be 39.75%. Some reasons for discrepancies between the theoretical and actual yields are trapped CO<sub>2</sub> and the formation of metal carbides.
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-In the TGA trace of calcium oxalate monohydrate, the first mass loss corresponds to loss of water of hydration.  The second mass loss corresponds to decomposition of dehydrated calcium oxalate to calcium carbonate and carbon monoxide and carbon dioxide.  The last mass loss is due to the decomposition of calcium carbonate to calcium oxide and carbon dioxide.
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-Figure 5 shows thermograms of four different chloro-polymers: (a) [[polyvinyl chloride]], (b) [[chlorinated polyvinyl chloride]], (c) chlorinated rubber, and (d) [[polyvinylidene chloride]].<ref name=ref7>{{cite journal | title = Carbonization of Polymers I - Thermogravimetric Analysis | journal = [[Polymer]] | year = 1962 | volume = 3 | pages = 1–10 | doi = | author1 = Gilbert, J. B. | author2 = Kipling, J. J. | author3 = McEnaney, B. | author4 = Sherwood, J. N.}}</ref> There are two stages of degradation in these four polymers. The first stage is the loss of [[hydrogen chloride]], and is complete around 250°C.  This first step occurs at lower temperatures for the polymers containing more chlorine (chlorinated polyvinyl chloride, chlorinated rubber, and polyvinylidene chloride), implying that these chloride groupings are less stable than in polyvinyl chloride.<ref name=ref7>{{cite journal | title = Carbonization of Polymers I - Thermogravimetric Analysis | journal = [[Polymer]] | year = 1962 | volume = 3 | pages = 1–10 | doi = | author1 = Gilbert, J. B. | author2 = Kipling, J. J. | author3 = McEnaney, B. | author4 = Sherwood, J. N.}}</ref>
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-The second stage is the [[carbonization]] of the polymer, and takes place between 250°C and 500°C. This is seen by the large loss of mass between 250°C and 500°C. Tar and simple gases, such as [[hydrogen]] and [[methane]], are evolved and the carbon that remains loses very little mass between 500°C and 900°C. In this second stage, the higher the chlorine content of the polymer, the lower the yield of tar. This is because chlorine is able to remove hydrogen, which would otherwise be used in the compounds that form tar.<ref name=ref7>{{cite journal | title = Carbonization of Polymers I - Thermogravimetric Analysis | journal = [[Polymer]] | year = 1962 | volume = 3 | pages = 1–10 | doi = | author1 = Gilbert, J. B. | author2 = Kipling, J. J. | author3 = McEnaney, B. | author4 = Sherwood, J. N.}}</ref>
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-==Thermal stability==
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-TGA can be used to evaluate the [[thermal stability]] of a material. In a desired temperature range, if a species is thermally stable, there will be no observed mass change. Negligible mass loss corresponds to little or no slope in the TGA trace. TGA also gives the upper use temperature of a material. Beyond this temperature the material will begin to degrade.
+ </ul>
-TGA has a wide variety of applications, including analysis of [[ceramic materials|ceramics]] and thermally stable polymers.  Ceramics usually melt before they decompose as they are thermally stable over a large temperature range, thus TGA is mainly used to investigate the thermal stability of polymers.  Most polymers melt or degrade before 200°C. However, there is a class of thermally stable polymers that are able to withstand temperatures of at least 300°C in air and 500°C in inert gases without structural changes or strength loss, which can be analyzed by TGA.<ref name=ref9>{{ cite journal | title = Synthesis of Thermally Stable Polymers | journal = [[Ft. Belvoir: Defense Technical Information Center]] | year = 1972 | author1 = Marvel, C. S.}}</ref> For example, the polyimide Kapton® loses less than 10% mass when held in 400°C air for 100 hours.<ref name=ref9>{{ cite journal | title = Synthesis of Thermally Stable Polymers | journal = [[Ft. Belvoir: Defense Technical Information Center]] | year = 1972 | author1 = Marvel, C. S.}}</ref>
-Figure 6 compares various high performance fibers using TGA as an evaluation of thermal stability. From the TGA, polyoxazole (PBO) has the highest thermal stability of the four fibers as it is stable up to ca. 500°C. [[Ultra-high-molecular-weight polyethylene]] (UHMW-PE) has the lowest thermal stability, as it begins to degrade around 200°C. Often the onset of mass loss is seen more prominently in the first derivative of the mass loss curve, as evidenced by Figure 2. High performance fibers used in bulletproof vests must remain strong enough mechanically so as to protect the user from incoming projectiles. The thermal and photochemical degradation of the fibers causes the mechanical properties of the vests to decrease, effectively rendering the armor useless. Thus, thermal stability is a key property when designing these vests.<ref name=ref8>{{cite journal | title = Evaluating the Thermal Stability of High Performance Fibers by TGA | journal = [[Journal of Applied Polymer Science]] | year = 2006 | volume = 99 | pages = 937–944 | doi = 10.1002/app.22305 | author1 = Liu, X. | author2 = Yu, W.}}</ref>
-Three ways a material can lose mass during heating are through chemical reactions, the release of adsorbed species, and decomposition.  All of these indicate that the material is no longer thermally stable. Out of the four fibers shown in Figure 6, only Terlon shows loss of adsorbed species, most likely water, as the mass loss occurs after 100°C. Because the TGA is performed in air, oxygen reacts with the organic fibers which eventually degrade completely, evidenced by the 100% mass loss. It is important to link thermal stability to the gas in which the TGA is performed. PBO, which completely decomposes when heated in air, retains ~60% mass when heated in N<sub>2</sub>.<ref name=ref10>{{cite journal | title = Synthesis and Characterization of Fluorinated PBO with High Thermal Stability and Low Dielectric Constant | journal = [[Journal of Macromolecular Science, Part B]] | year = 2009 | volume = 48 | pages = 1114–1124 | doi = 10.1080/00222340903041244 | author1= Tao, Z. | author2 = Jin, J. | author3 = Yang, S. | author4 = Hu, D. | author5 = Li, G. | author6 = Jiang, J.}}</ref> Thus, PBO is thermally stable in nitrogen up to 630°C, whereas in air, PBO has almost completely decomposed at that temperature.
-==Oxidation processes==
-Oxidative mass losses are the most common observable losses in TGA.<ref name=ref11>{{cite journal | title = The Effect of Purity on High-Temperature Oxidation of Zirconium | journal = [[Oxidation of Metals]] | year = 1994 | volume = 42 | pages = 223–237 | doi = 10.1007/BF01052024 | author1 = Voitovich, V. B. | author2 = Lavrenko, V. A. | author3 = Voitovich, R. F. | author4 = Golovko, E. I.}}</ref> Figure 7 shows the mass gain  vs. temperature for three [[copper alloys]]. All of the mass gain of these alloys is due to oxidation. The histogram also includes the mass gain of copper alone.<ref name=ref12>{{cite journal | title = Comparison of the Oxidation Rates of Some New Copper Alloys | journal = [[Oxidation of Metals]] | year = 2003 | volume = 60 | pages = 271–291 | doi = 10.1023/A:1026019202691 | author1 = Ogbuji, L. U. | author2 = Humphrey, D. L.}}</ref> The composition of the GR-84 alloy is 8 wt.% Cu, 4 wt.% Cr and the remainder is Nb. The composition of the GC-15 alloy is copper with 0.15wt.% Al. The composition of the NAR-Z alloy is Cu-3 wt.% Al-0.5 wt.% Zr. This last alloy was the liner of the main engine of the space shuttle in 2005.<ref name=ref12>{{cite journal | title = Comparison of the Oxidation Rates of Some New Copper Alloys | journal = [[Oxidation of Metals]] | year = 2003 | volume = 60 | pages = 271–291 | doi = 10.1023/A:1026019202691 | author1 = Ogbuji, L. U. | author2 = Humphrey, D. L.}}</ref>
-Studying the resistance to oxidation in copper alloys is very important. For example, [[NASA]] (National Aeronautics and Space Administration) is conducting research on advanced copper alloys for their possible use in [[combustion engines]]. However, oxidative degradation can occur in these alloys as copper oxides form in atmospheres that are rich in oxygen. Resistance to oxidation is very important because NASA wants to be able to reuse shuttle materials. TGA can be used to study the static oxidation of materials such as these for practical use.
-Some researchers have been studying ways in which to protect certain [[oligomers]] or polymers from oxidation processes. One example is inserting an oligomer into a multi[[block copolymer]].<ref name=ref13>{{cite journal | title = Thermogravimetric investigation of two classes of block copolymers based on poly(lactic-glycolic acid) and poly(ε-caprolactone) or poly(ethylene glycol) | journal = [[Polymer Degradation and Stability]] | year = 2001 | volume = 74 | pages = 119–124 | doi = 10.1016/S0141-3910(01)00110-0 | author1 = D'Antone, S. | author2 = Bignotti, F. | author3 = Sartore, L. | author4 = D’Amore, A. | author5 = Spagnoli, G. | author6 = Penco, M.}}</ref> The TGA traces of both the oligomer and the oligomer/multiblock copolymer in N<sub>2</sub> and in air are shown in Figure 8.<ref name=ref13>{{cite journal | title = Thermogravimetric investigation of two classes of block copolymers based on poly(lactic-glycolic acid) and poly(ε-caprolactone) or poly(ethylene glycol) | journal = [[Polymer Degradation and Stability]] | year = 2001 | volume = 74 | pages = 119–124 | doi = 10.1016/S0141-3910(01)00110-0 | author1 = D'Antone, S. | author2 = Bignotti, F. | author3 = Sartore, L. | author4 = D’Amore, A. | author5 = Spagnoli, G. | author6 = Penco, M.}}</ref> When the TGAs were run under a nitrogen atmosphere (Figure 8a and b), there is no oxidation of the substrate. When the TGA of the oligomer was run under air (Figure 8c), an oxidation process can be seen between 200°C-350°C. This process is not seen for the oligomer/multiblock copolymer (Figure 8d). The authors of this paper explained this disappearance by suggesting that the oxidative process involved [[hydroxyl]] end groups on the oligomer. The encasing of the oligomer by the multiblock copolymer prevented this from happening.<ref name=ref13>{{cite journal | title = Thermogravimetric investigation of two classes of block copolymers based on poly(lactic-glycolic acid) and poly(ε-caprolactone) or poly(ethylene glycol) | journal = [[Polymer Degradation and Stability]] | year = 2001 | volume = 74 | pages = 119–124 | doi = 10.1016/S0141-3910(01)00110-0 | author1 = D'Antone, S. | author2 = Bignotti, F. | author3 = Sartore, L. | author4 = D’Amore, A. | author5 = Spagnoli, G. | author6 = Penco, M.}}</ref>
-==Combustion==
-Combustion during TG analysis is identifiable by distinct traces made in the TGA thermograms produced.  One interesting example occurs with samples of as-produced unpurified [[carbon nanotubes]] that have a large amount of metal [[catalyst]] present (See Figure 9). Due to combustion, a TGA trace can deviate from the normal form of a well-behaved function. This phenomenon arises from a rapid temperature change.  When the weight and temperature are plotted versus time, a dramatic slope change in the first derivative plot is concurrent with the mass loss of the sample and the sudden increase in temperature seen by the thermocouple. The mass loss could be the result of particles of smoke released from burning caused by inconsistencies in the material itself, beyond the oxidation of carbon due to poorly controlled weight loss.
-==References==
-{{reflist}}
-{{DEFAULTSORT:Thermogravimetric Analysis}}
-[[Category:Thermodynamics]]
-[[Category:Materials science]]

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